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Integrated measurements of capillary pressure, electrical resistivity, and elastic wave velocities conducted during sample drainage and imbibition under simulated reservoir conditions.

Understanding how fluids migrate through underground rock formations is essential for securely storing carbon dioxide ($CO_2$), managing groundwater resources, or cleaning up contaminated soils. A key parameter in this context is the capillary pressure, the pressure difference between two immiscible fluids, such as water and $CO_2$, in the pore space of rocks. However, reliable measurements of capillary pressure under realistic subsurface conditions are still limited. Capillary pressure–saturation relationships were determined using the porous membrane technique within a custom-designed experimental platform SEPP (System for Experimental PetroPhysics) developed at GFZ Helmholtz Centre for Geosciences. Measurements were conducted during both drainage and imbibition cycles under pressure and temperature conditions relevant for subsurface $CO_2$ storage reservoirs. SEPP enables integrated acquisition of key petrophysical parameters, including hydraulic, electrical, and elastic properties. This data publication presents two datasets capturing capillary pressure, electrical resistivity, and P- and S-wave velocities from tests on two distinct sandstone samples.

Crystal Size Distribution Analyses of Isothermal Deformation Experiments

In this work we aimed to investigate and quantify the relative importance of dynamic conditions (e.g., stirring in a Concentric Cylinder apparatus) on the crystallization kinetics of basaltic magmas (Stromboli). This was achieved by observing the final textures of the samples, analysing the resulting SEM images, and finally relating the resulting parameters to specific growth and nucleation rates. The dataset is made of: 1) A folder called "SEM Images" with two sub-folders inside, representative of the two experiments carried out, called "CG1" and "CG2.3" 2) An Excel file, consisting in 4 data sheets, where all results of image analysis are included, divided in sections. The sheets are also available in CSV format. This publication results from work conducted under the transnational access/national open access action at High Pressure - High Temperature Laboratory (HPHT Lab), Istituto Nazionale di Geofisica e Vulcanologia (INGV), Rome, Italy supported by WP3 ILGE - MEET project, PNRR - EU Next Generation Europe program, MUR grant number D53C22001400005.

3D textural characterization of rocks representing S. Miguel Island (Azores, Portugal)

The role of the physical and microstructural properties of lavas impacts the dynamics of magma ascent and of the volcanic edifice itself. In the context of a doctoral project, ten samples representative of the central volcanoes of S. Miguel Island (Azores, Portugal), priorily collected in available outcrops in the island, were microstructurally assessed for the first time in the INGV-OV (Naples). Imaging was processed by the ZEISS Xradia Versa 410 X-ray computed microtomography. This tool enables accurate and complete textural characterization of rocks by providing 3D images of the samples. Posteriorly, the rocks were analysed with a dedicated image analysis software to resolve the internal microstructure of the samples. determining several key properties (porosity, permeability, fracturation, and crystal content) that are of major relevance for a posterior physical and mechanical assessment. This publication results from work conducted under the transnational access/national open access action at magLab, INGV-OV (Naples, Italy) supported by WP3 ILGE - MEET project, PNRR - EU Next Generation Europe program, MUR grant number D53C22001400005.

Multi-collector 40Ar/39Ar data of glass and plagioclase from a tuff sample in the marine claystone of the Argille di Spadafora (NE Sicily, Italy)

The dataset contain full 40Ar/39Ar geochronological data completed by multi collector noble gas mass spectrometry on plagioclase and glass separates from a tuff sample interbedded in Pleistocene marine claystone (Argille di Spadafora) of northeastern Sicily (Italy). Tuff unit VU7 was identified in the field using the published base map and stratigraphic nomenclature of Di Bella et al. (2016), which correlates to bathyal marine marl (Argille di Vito Superiore) in southern Calabria. The tuff contains stratified white lapilli with abundant fresh volcanic glass shards and was deposited by a submarine turbidity current from a single volcanic eruption. The Ar laserprobe facility was realized with the financial support of CNR. The CO2 laser system was acquired within the PNRR – Mission 4, “Education and Research” - Component 2, “From research to business” - Investment line 3.1, “Fund for the creation of an integrated system of research and innovation infrastructures” - Project IR0000025 MEET. EPOS JRU Italia is acknowledged for support in the Laboratory maintenance.

Carbon isotopes in OIB Mantle source

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Microstructure and mechanical properties of massive and porous of lavas from S. Miguel Island (Azores, Portugal)

The role of elongated pores and crystals of lavas influences their mechanical and physical behaviour, providing a first microstructural clue. In the context of a doctoral project, two samples – a trachyte and a basalt/andesite (s.l.) - representative of Fogo Volcano (S. Miguel Island, Azores, Portugal) were collected as part of an intact rock study. They were microstructurally assessed in the INGV-OV (Naples) using the ZEISS Xradia Versa 410 X-ray computed microtomography to obtain high-resolution 3D images, as well as to perform real-time in-situ mechanical tests (uniaxial – 7 mm diameter cylinders - and Brazilian – 13 mm diameter discs) to assess how elongated pores/crystals control strength. In addition to 3D images of the samples, which allow segmentation of the pore space and crystals, mechanical tests show that trachytes are more competent than vesicular basalts/andesites. Both pores and crystals control the development of the crack pattern.

CAMSIZER Particle Size Data from Explosive Paroxysms of Mt. Etna (2011–2025)

Mt. Etna in Catania, Italy, is an active volcano that has served as a natural laboratory for many volcanologists worldwide. Its paroxysms are unique eruptive events caused by a complex magmatic system that, despite being one of the most studied volcanoes, there is still an open field to contribute to the understanding of magma dynamics and degassing. This data set is a compilation of grain-size and shape measurements of 14 tephra samples of Mt. Etna. The tephra samples correspond to some of the most explosive cycles and events of the volcano from 2011 to 2025. The measurements were obtained using CAMSIZER through the ILGE TNA grant funding at INGV sezione di Catania. This dataset is the basis for a research project investigating the controls on the volume of gases and magma emitted during an eruption of Mt. Etna. This publication results from work conducted under the transnational access/national open access action at Sedimentology Laboratory – INGV sezione di Catania supported by WP3 ILGE - MEET project, PNRR - EU Next Generation Europe program, MUR grant number D53C22001400005.

Trace element concentration of minerals in the Morro São João malignites (Serra do Mar, Brazil)

The Morro São João intrusion is located in the easternmost part of the Serra do Mar province, along the Cabo Frio lineament (Fig. 1) and has an area of approximately 10 km². It is a Late Cretaceous intrusion formed by clinopyroxenites, melagabbros, shonkinites, malignites, nepheline syenites, and phonolite dikes, without olivine, and is thought to have formed by closed system crystallization of a fairly evolved tephritic melt of potassic/ultrapotassic affinity (cf. Brotzu et al., 2007). We have analyzed two malignites, and specifically, their liquidus phases (clinopyroxene, titanite, garnet, amphibole). Analyzing the trace elements in these minerals helps us to better understand the different fractionation of the elements in these coexisting phases, and the implications for the evolution processes that occurred in the Morro São João magma reservoir. These analyses also provided important information about the concentration of rare earth elements (REEs) and high field strength elements (HFSEs), and their change with the magmatic evolution of the suite. This publication results from work conducted under the transnational access/national open access action at Mass spectrometry la-icp laboratory (IGG-CNR, Italy) supported by WP3 ILGE - MEET project, PNRR - EU Next Generation Europe program, MUR grant number D53C22001400005.

Rheology of PDMS Korasilon G20OH (#1000039264) used at the Laboratory for Experimental Tectonics at GFZ Helmholtz Centre for Geosciences, Potsdam, Germany

This dataset provides rheometric data of the PDMS Korasilon G 20 OH used for analogue modelling at the Laboratory for Experimental Tectonics at GFZ Helmholtz Centre for Geosciences, Potsdam, Germany. The batch number is 1000039264, purchased in 2022 and opened in 2026. The material sample has been analyzed at the Laboratory for Experimental Tectonics at GFZ Helmholtz Centre for Geosciences, Potsdam (HelTec) using an Anton Paar Physica MCR 301 rheometer in a cone-plate configuration at room temperature (21˚C). Rotational (controlled shear rate) tests with shear rates varying from 10^-4 to 10^-1 s^-1 were performed. According to our rheometric analysis, the material is quasi-Newtonian (n~1) at strain rates below 10^-2 s^-1 and weakly shear rate thinning above. The viscosity of G 20 OH is 1.8*10^4 Pa s.

Horizontal-to-Vertical Spectral Ratios (HVSR) of NW Italy seismic stations elaborated during the "FOCUS-HVNEA" NOA-ILGE project

This data set consists of Horizontal-to-Vertical Spectral Ratios (HVSR) resulting from the application of the software package HVNEA (HV Noise and Earthquake Automatic Analysis) with the aim of comparing them with those resulting from the application of another method, namely STATION (Seismic sTATion and sIte amplificatiON). The results, relative to more than 24,000 HVSR, derive from the processing of 700,000 seismograms recorded over different time periods by 8 stations of the networks IV (Italian Seismic Network), GU (Regional Seismic Network of North Western Italy) and GV (Mobile RSNI). To compare the results of the two methods as accurately as possible, the waveforms were subjected to the same preprocessing already used to elaborate the results stored in the STATION database. To this end, the methodological workflow applied with HVNEA for station IV.MURB involved the selection of segments from continuous recordings for each event reported in the INGV catalogue located within a radius of 120 kilometres from the station. Starting from the automatically picked S-wave onsets, 12-second windows were then extracted and used for the analysis of earthquake recordings. Regarding the noise analysis, it should be noted that STATION again considers 12-second windows selected before the P-wave onset, while HVNEA requires the use of a signal window of at least 60 seconds. A window of 3,600 seconds was used for the analysis. The comparison of the HVSR was performed in the frequency band 0.1–15 Hz. All analysed curves, for both earthquake and noise recordings, show generally similar shapes and identify significant peaks in correspondence of the same frequency ranges, although the amplitudes obtained with STATION are systematically higher than those obtained with HVNEA. To obtain a quantitative comparison, various statistical metrics commonly used to measure the discrepancy between data sets were applied, namely the Mean Squared Error, the Mean Absolute Error and the Pearson Correlation Coefficient. This publication results from work conducted under the transnational access/national open access action at the Site effects Laboratory – INGV L’Aquila supported by WP3 ILGE–MEET project, PNRR–EU Next Generation Europe program, MUR grant number D53C22001400005.

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