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The role of the physical and microstructural properties of lavas impacts the dynamics of magma ascent and of the volcanic edifice itself. In the context of a doctoral project, ten samples representative of the central volcanoes of S. Miguel Island (Azores, Portugal), priorily collected in available outcrops in the island, were microstructurally assessed for the first time in the INGV-OV (Naples). Imaging was processed by the ZEISS Xradia Versa 410 X-ray computed microtomography. This tool enables accurate and complete textural characterization of rocks by providing 3D images of the samples. Posteriorly, the rocks were analysed with a dedicated image analysis software to resolve the internal microstructure of the samples. determining several key properties (porosity, permeability, fracturation, and crystal content) that are of major relevance for a posterior physical and mechanical assessment. This publication results from work conducted under the transnational access/national open access action at magLab, INGV-OV (Naples, Italy) supported by WP3 ILGE - MEET project, PNRR - EU Next Generation Europe program, MUR grant number D53C22001400005.
This data publication is supplementary to a study on microbial weathering of Fe-bearing minerals in the deep biosphere of a semi-arid environment (Chile). The dataset contains mineralogical, geochemical, microbiological and thermodynamic data of an 87 m deep drill core profile located in the Chilean Coastal Cordillera (Santa Gracia (SG)). The drilling campaign was conducted in March-April 2019 as part of the German Science Foundation (DFG) priority research program SPP 1803 “EarthShape: Earth Surface Shaping by Biota”. The project focused on how microorganisms contribute to mineral weathering and thus shape Earth´s surface. Aim of the drilling campaign was to recover the continuous weathering profile from surface to weathering front and to pinpoint as well as disentangle weathering processes at depth. For this purpose, extractable Fe pools, water-extractable organic carbon and nitrate, energy yields of Fe redox reactions, in situ microbial Fe(III) reduction, microbial Fe(III) reduction extent in microcosms, as well as community compositions of in situ and microcosms derived 16S rRNA gene amplicon sequence variants (ASVs) were determined.
The role of elongated pores and crystals of lavas influences their mechanical and physical behaviour, providing a first microstructural clue. In the context of a doctoral project, two samples – a trachyte and a basalt/andesite (s.l.) - representative of Fogo Volcano (S. Miguel Island, Azores, Portugal) were collected as part of an intact rock study. They were microstructurally assessed in the INGV-OV (Naples) using the ZEISS Xradia Versa 410 X-ray computed microtomography to obtain high-resolution 3D images, as well as to perform real-time in-situ mechanical tests (uniaxial – 7 mm diameter cylinders - and Brazilian – 13 mm diameter discs) to assess how elongated pores/crystals control strength. In addition to 3D images of the samples, which allow segmentation of the pore space and crystals, mechanical tests show that trachytes are more competent than vesicular basalts/andesites. Both pores and crystals control the development of the crack pattern.
In this work we aimed to investigate and quantify the relative importance of dynamic conditions (e.g., stirring in a Concentric Cylinder apparatus) on the crystallization kinetics of basaltic magmas (Stromboli). This was achieved by observing the final textures of the samples, analysing the resulting SEM images, and finally relating the resulting parameters to specific growth and nucleation rates. The dataset is made of: 1) A folder called "SEM Images" with two sub-folders inside, representative of the two experiments carried out, called "CG1" and "CG2.3" 2) An Excel file, consisting in 4 data sheets, where all results of image analysis are included, divided in sections. The sheets are also available in CSV format. This publication results from work conducted under the transnational access/national open access action at High Pressure - High Temperature Laboratory (HPHT Lab), Istituto Nazionale di Geofisica e Vulcanologia (INGV), Rome, Italy supported by WP3 ILGE - MEET project, PNRR - EU Next Generation Europe program, MUR grant number D53C22001400005.
The Jacupiranga carbonatite (Brazil) was investigated to better understand how modal proportions and mineral chemistry control the fO2 recorded by a natural carbonatite rock. Mineral compositions were determined using SEM-EDS, EPMA-WDS and Raman microspectroscopy building upon detailed petrography. Based on magnetite-ilmenite oxythermobarometry, rock-forming temperatures range from 505 to 732 °C, with a wide span of fO2 values (∆FMQ –1.21 to +4.56). In each sample, ilmenite grains and lamellae are distinguishable, with the latter recording higher temperature–fO2 conditions. Consistently, independently determined homogenization temperatures of apatite-hosted fluid inclusions show a similar range between 550 and 685 °C. From the wall-rock contact toward the carbonatite body, samples exhibit a decrease in the modal abundance of olivine, phlogopite, magnetite, ilmenite, and dolomite, alongside an increase in Mg-calcite. Over the same spatial gradient, temperature, fO2, and the magnesioferrite (in magnetite) and geikielite (in ilmenite) components decrease. During the antiskarn reaction, silica and mafic components (Mg, FeT, Al, and Ti) derived from the ultramafic wall-rock were incorporated into olivine, phlogopite, magnetite-ilmenite, and dolomite. Calcite-rich samples, which were less influenced by the wall-rock, preserved ephemeral alkali components of the carbonatite melts within burbankite. Apatite-hosted fluid inclusions represent coeval fluid modified by antiskarn reactions. Adjacent to equilibrium magnetite-ilmenite pairs, olivine and phlogopite exhibit high mg# (93–97 and 88–95, respectively). Despite the broad span of ∆FMQ values recorded by the oxide pairs, we found only a weak positive correlation between the recorded fO2 and mg#. Consequently, we suggest that the high mg# (>88–90) of carbonatitic olivine is primarily controlled by the low (<0.2) 〖K_D〗_(Fe^(2+)-Mg)^(olivine-carbonatite melt) (Fe2+/Mg exchange partition coefficient between olivine and the carbonatite melt) at crustal conditions. The exceptionally high mg# of olivine and phlogopite, compared to the adjacent dunite cumulates (mg# 84–88), combined with their negligible Ni and Cr contents, indicate an in situ antiskarn process. This study demonstrates that carbonatite systems can be characterized by dynamic redox conditions, spanning the range from Fe3O4 ̶ Fe2O3 to Fe2SiO4 ̶ Fe3O4 ̶ SiO2 during their evolution and emplacement.
This dataset presents a comprehensive geochemical and petrological record for the Hujialin ultramafic body in the Sulu orogenic belt, a major ultrahigh-pressure terrane in eastern China. The data compilation includes mineral proportions (Table S1), whole-rock major and trace element compositions (Table S2), whole-rock Sr–Nd isotopic ratios (Table S3), major and trace element compositions of olivine (Table S4), spinel (Table S5), garnet (Table S6), and clinopyroxene (Table S7), oxygen isotope compositions of whole-rock and mineral separates (Table S8), and modeled melt–cumulate compositions using the MELTS algorithm (Table S9). The dataset integrates newly acquired analyses with previously published data for several garnet-rich clinopyroxenites, allowing a unified comparison across the Hujialin ultramafic suite. This study was supported by funds from National Key Research and Development Program of China (2024YFF0807300) and the Fundamental and Interdisciplinary Disciplines Breakthrough Plan of the Ministry of Education of China (JYB2025XDXM911).
This dataset presents the raw data from one experimental series (named CCEX, i.e., Caldera Collapse under regional Extension) of analogue models performed to investigate the process of caldera collapse followed by regional extension. Our experimental series tested the case of perfectly circular collapsed calderas afterward stretched under regional extensional conditions, that resulted in elongated calderas. The models are primarily intended to quantify the role of regional extension on the elongation of collapsed calderas observed in extensional settings, such as the East African Rift System. An overview of the performed analogue models is provided in Table 1. Analogue models have been analysed quantitatively by means of photogrammetric reconstruction of Digital Elevation Model (DEM) used for 3D quantification of the deformation, and top-view photo analysis for qualitative descriptions. The analogue materials used in the setup of these models are described in Montanari et al. (2017), Del Ventisette et al. (2019), Bonini et al., 2021 and Maestrelli et al. (2021a,b).
This data report presents the in-situ LA-ICP-MS trace element composition of sphalerite, pyrite, and chalcopyrite from the Aouli Ag-Pb-Zn-(Cu) vein system in the Upper Moulouya district, Morocco. The dataset contributes to a study focused on characterizing the element concentrations in sulfides and elucidating the ore-forming processes at the Aouli deposit. Located within the Hercynian inlier of the Upper Moulouya, this deposit hosts one of Morocco’s largest argentiferous Pb-Zn ± F ± Ba vein-type deposits. The mineralization occurs within polyphase hydrothermal veins, oriented NE-SW to E-W and WNW-ESE. These veins occur as lodes, ore shoots, or discontinuous vein infill, with their emplacement largely controlled by structural intersections. The deposit hosts a complex mineralogical assemblage, including Ni-Co-Fe arsenides and sulfarsenides, Pb-Zn-Cu sulfides, and Ag-Sb-As sulfosalts occurring in the same vein structures, which are described for the first time. Consequently, the characterization of pyrite, chalcopyrite, and particularly sphalerite will help constrain the ore-forming process and determine the physicochemical conditions (T–fS2) of the mineralizing fluids.
The study of textural and chemical characteristics of mafic minerals from mantle xenoliths is essential to investigate the nature of the upper mantle in a continental geodynamic context, melts generation and their effects related to mantle metasomatism. Particular textures in mantle minerals, inclusions or secondary veins of different nature (silicates vs carbonates), bubbles, represent petrographic tools to investigate these processes within the mantle. Petrographic 2D thin sections might overlook these mineralogical features, and 3D textural analysis through X-ray computed microtomography (micro-CT) are crucial to overcome these limitations. We focused on the Mt. Vulture volcano (southern Italy) rare mantle xenoliths, brought to the surface by a melilitite-carbonatite magma (141 ka), with particular emphasis to spinel-wehrlite xenoliths and wehrlitization processes that is located close to an area of intense CO2 degassing associated to catastrophic earthquakes. Preliminary results showed interesting 3D textural distributions within the studied xenoliths-forming mantle minerals. In particular, the micro-CT allowed to furnish new constrains on the relationship between fluids entrapment and migration, and structural discontinuities. Indeed, some minerals (especially those from the wehrlite xenoliths) showed a well-correlated distribution of fluid inclusions along the secondary fracturing planes. This publication results from work conducted under the transnational access/national open access action at Istituto Nazionale di Geofisica e Vulcanologia – Osservatorio Vesuviano (INGV-OV) and supported by WP3 ILGE - MEET project, PNRR - EU Next Generation Europe program, MUR grant number D53C22001400005. The author thanks also Gianmarco Buono and Lucia Pappalardo for their support during the analyses and the post processing process.
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